6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine

Base Information

Chemical Name:6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine
CAS No.:212391-51-0
Molecular Formula:C₁₅H₁₂Cl₂N₄OS
Molecular Weight:367.258
Hs Code.:

Synonyms:6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine

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Chemical Property of 6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine

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Technology Process of 6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine

There total 5 articles about 6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 185039-29-6
6-(2,6-Dichlorophenyl)-8-methyl-2-methylsulfanyl-8H-pyrido[2,3-d]-pyrimidin-7-ylideneamine

: 212391-51-0
6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine

Guidance literature:: With N-(benzenesulfonyl)-3-phenyloxaziridine; In chloroform; Ambient temperature;
DOI:10.1021/jm9802259

Reference yield:

: 5909-24-0
4-chloro-2-methanesulfanylpyrimidine-5-carboxylic acid ethyl ester

: 212391-51-0
6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / Et₃N / tetrahydrofuran; H₂O / 0.5 h / 25 °C

2: 84 percent / LiAlH₄ / tetrahydrofuran / 0.17 h / Ambient temperature

3: 93 percent / MnO₂ / CHCl₃ / 6 h / Ambient temperature

4: 46 percent / K₂CO₃ / dimethylformamide / 18 h / 100 - 105 °C

5: 73 percent / 3-phenyl-2-(phenylsulfonyl)oxaziridine / CHCl₃ / Ambient temperature

With manganese(IV) oxide; lithium aluminium tetrahydride; potassium carbonate; N-(benzenesulfonyl)-3-phenyloxaziridine; triethylamine; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jm9802259

Reference yield:

: 17759-30-7
(4-methylamino-2-methylsulfanyl-pyrimidin-5-yl)-methanol

: 212391-51-0
6-(2,6-Dichloro-phenyl)-2-methanesulfinyl-8-methyl-8H-pyrido[2,3-d]pyrimidin-7-ylideneamine

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / MnO₂ / CHCl₃ / 6 h / Ambient temperature

2: 46 percent / K₂CO₃ / dimethylformamide / 18 h / 100 - 105 °C

3: 73 percent / 3-phenyl-2-(phenylsulfonyl)oxaziridine / CHCl₃ / Ambient temperature

With manganese(IV) oxide; potassium carbonate; N-(benzenesulfonyl)-3-phenyloxaziridine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm9802259