pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Base Information

Chemical Name:pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide
CAS No.:1373545-44-8
Molecular Formula:C₂₃H₂₂N₄O₂S
Molecular Weight:418.519
Hs Code.:

Synonyms:pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

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Chemical Property of pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

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Technology Process of pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

There total 4 articles about pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16133-25-8
Pyridine-3-sulfonyl chloride

: 1373546-48-5
2-(2-aminophenyl)-4,4-dimethyl-1,2,3,4-tetrahydroquinoline-6-carbonitrile

: 1373545-44-8
pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: With pyridine; at 20 ℃; for 3h; Inert atmosphere; Cooling with ice;

Reference yield:

: 1373546-47-4
4,4-dimethyl-2-(2-nitrophenyl)-1,2,3,4-tetrahydroquinoline-6-carbonitrile

: 1373545-44-8
pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; iron / ethanol; water / 3 h / Inert atmosphere; Reflux

2: pyridine / 3 h / 20 °C / Inert atmosphere; Cooling with ice

With pyridine; iron; ammonium chloride; In ethanol; water;

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 1373545-44-8
pyridine-3-sulfonic acid N-[2-(6-cyano-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-2-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: ethanol / 3 h / Reflux

2: boron trifluoride diethyl etherate / 90 °C

3: ammonium chloride; iron / ethanol; water / 3 h / 20 °C / Reflux; Inert atmosphere

4: pyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere; Cooling with ice

With pyridine; boron trifluoride diethyl etherate; iron; ammonium chloride; In ethanol; dichloromethane; water;