α,α-dideuteriodibenzyl ether

Base Information

Chemical Name:α,α-dideuteriodibenzyl ether
CAS No.:75163-12-1
Molecular Formula:C₁₄H₁₄O
Molecular Weight:200.249
Hs Code.:

Synonyms:α,α-dideuteriodibenzyl ether

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Chemical Property of α,α-dideuteriodibenzyl ether

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Technology Process of α,α-dideuteriodibenzyl ether

There total 3 articles about α,α-dideuteriodibenzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 21175-64-4
1,1-dideuteriophenylmethanol

: 100-39-0
benzyl bromide

: 75163-12-1
α,α-dideuteriodibenzyl ether

Guidance literature:: With sodium hydride; In 1,2-dimethoxyethane; 1.) 2 h, 2.) reflux, 20 min;
DOI:10.1021/ja00531a030

Reference yield:

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 75163-12-1
α,α-dideuteriodibenzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 2.0 g / LiAlD₄ / diethyl ether / 2 h / Heating

2: 51 percent / sodium hydride / 1,2-dimethoxy-ethane / 1.) 2 h, 2.) reflux, 20 min

With lithium aluminium deuteride; sodium hydride; In 1,2-dimethoxyethane; diethyl ether;
DOI:10.1021/ja00531a030

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 75163-12-1
α,α-dideuteriodibenzyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlD₄

2: potassium hydroxide / dimethylsulfoxide

With potassium hydroxide; lithium aluminium deuteride; In dimethyl sulfoxide;
DOI:10.1002/oms.1210161003