C₃₂H₅₀O₉Si

Base Information

Chemical Name:C₃₂H₅₀O₉Si
CAS No.:250577-76-5
Molecular Formula:C₃₂H₅₀O₉Si
Molecular Weight:606.829
Hs Code.:

C<sub>32</sub>H<sub>50</sub>O<sub>9</sub>Si

Synonyms:C₃₂H₅₀O₉Si

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Chemical Property of C₃₂H₅₀O₉Si

Chemical Property:

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Technology Process of C₃₂H₅₀O₉Si

There total 20 articles about C₃₂H₅₀O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 250577-77-6
C₃₁SiH₄₀O₄

: 250577-76-5
C₃₂H₅₀O₉Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

2.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

3.1: 3.39 g / toluene / 1 h / 70 °C

4.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

4.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

5.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

6.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

7.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

8.1: 98 percent / benzene / 14 h / Heating

9.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

9.2: 78 percent / tetrahydrofuran / -78 - 20 °C

10.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

With oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; acetone; toluene; benzene; 2.1: Swern oxidation / 3.1: Wittig olefination / 4.2: Wittig olefination / 10.1: Wittig olefination;
DOI:10.1021/ol990281j

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 250577-76-5
C₃₂H₅₀O₉Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 98 percent / imidazole / dimethylformamide / 0.5 h / 20 °C

2.1: 75 percent / H₂ / Pd/C / ethanol / 24 h / 2068.65 Torr

3.1: dimethyl sulfoxide; oxalyl chloride; ethyldiisopropylamine / CH₂Cl₂ / 0.92 h / -78 - 20 °C

4.1: 3.39 g / toluene / 1 h / 70 °C

5.1: sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

5.2: 82 percent / tetrahydrofuran / 0.58 h / -78 - 20 °C

6.1: 73 percent / diisobutylaluminum hydride / CH₂Cl₂; hexane / -78 - 0 °C

7.1: triethylamine / CH₂Cl₂ / 0 - 20 °C

8.1: 3.53 g / sodium iodide / acetone / 2 h / Heating

9.1: 98 percent / benzene / 14 h / Heating

10.1: sodium hexamethyldisilazide / tetrahydrofuran / 1 h / -78 °C

10.2: 78 percent / tetrahydrofuran / -78 - 20 °C

11.1: 90 mg / benzene; CH₂Cl₂ / 120 h / 20 °C

With 1H-imidazole; oxalyl dichloride; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; benzene; 3.1: Swern oxidation / 4.1: Wittig olefination / 5.2: Wittig olefination / 11.1: Wittig olefination;
DOI:10.1021/ol990281j

Reference yield:

: 250577-66-3
C₁₉H₃₇SiPO₆

: 250577-65-2
C₁₇H₂₄O₇

: 250577-76-5
C₃₂H₅₀O₉Si

Guidance literature:: C₁₉H₃₇SiPO₆; With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃; for 0.25h;

C₁₇H₂₄O₇; In tetrahydrofuran; at 20 ℃; for 16h; Further stages.;
DOI:10.1021/ol990281j