N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide

Base Information

Chemical Name:N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide
CAS No.:1064681-05-5
Molecular Formula:C₂₈H₂₀N₂O₆S
Molecular Weight:512.543
Hs Code.:

Synonyms:N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide

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Chemical Property of N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide

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Technology Process of N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide

There total 5 articles about N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1365958-54-8
N-(3-(2-methoxy-6-(3-methoxyphenyl)naphthalen-1-yl)phenyl)4-nitrobenzenesulfonamide

: 1064681-05-5
N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 18h;
DOI:10.1021/jm201735j

Reference yield:

: 1064680-92-7
1-(3-aminophenyl)-6-(3-hydroxyphenyl)naphthalen-2-ol

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1064681-05-5
N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide

Guidance literature:: 1-(3-aminophenyl)-6-(3-hydroxyphenyl)naphthalen-2-ol; 4-Nitrobenzenesulfonyl chloride; With polystyrene supported morpholine; In tetrahydrofuran; at 20 ℃; for 15h;

With polystyrene supported dimethylaminopyridine; In tetrahydrofuran; at 60 ℃; for 15h;
DOI:10.1021/jm201735j

Reference yield:

: 1041115-67-6
1-bromo-2-methoxy-6-(3-methoxyphenyl)naphthalene

: 1064681-05-5
N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)-4-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; ethanol; water / 0.25 h / 150 °C / 1125.11 Torr / Microwave irradiation

2.1: boron tribromide / dichloromethane / 18 h / -78 - 20 °C

3.1: polystyrene supported morpholine / tetrahydrofuran / 15 h / 20 °C

3.2: polystyrene supported dimethylaminopyridine / 15 h / 60 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; caesium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 1.1: Suzuki coupling;
DOI:10.1021/jm201735j