tricarbonyl[(2-5-η)-2-(4-methoxycyclohexa-2,4-dien-1-ylidene)-1-phenylethanol]iron

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Chemical Name:tricarbonyl[(2-5-η)-2-(4-methoxycyclohexa-2,4-dien-1-ylidene)-1-phenylethanol]iron
CAS No.:203914-40-3
Molecular Formula:C₁₈H₁₆FeO₅
Molecular Weight:368.169
Hs Code.:

Synonyms:tricarbonyl[(2-5-η)-2-(4-methoxycyclohexa-2,4-dien-1-ylidene)-1-phenylethanol]iron

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Chemical Property of tricarbonyl[(2-5-η)-2-(4-methoxycyclohexa-2,4-dien-1-ylidene)-1-phenylethanol]iron

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Technology Process of tricarbonyl[(2-5-η)-2-(4-methoxycyclohexa-2,4-dien-1-ylidene)-1-phenylethanol]iron

There total 1 articles about tricarbonyl[(2-5-η)-2-(4-methoxycyclohexa-2,4-dien-1-ylidene)-1-phenylethanol]iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 86664-11-1
tricarbonyl[(1-4-η)-2-methoxy-5-methylenecyclohexa-1,3-diene]iron

: 100-52-7
benzaldehyde

: 203914-40-3
tricarbonyl[(2-5-η)-2-(4-methoxycyclohexa-2,4-dien-1-ylidene)-1-phenylethanol]iron

Guidance literature:: With boron trifluoride diethyl etherate; triethylamine; In dichloromethane; N2-atmosphere; stirring PhC(O)H nad BF3*Et2O (30 min), addn. of soln. ofFe-compd. Et3N addn., stirring (30 min); water addn., extn. (CH2Cl2), chromy. (SiO2, hexane/EtOAc 4/1);
DOI:10.1021/om970684s