ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate

Base Information

Chemical Name:ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate
CAS No.:1200041-09-3
Molecular Formula:C₁₉H₂₉NO₅
Molecular Weight:351.443
Hs Code.:

Synonyms:ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate

Chemical Property:

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Technology Process of ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate

There total 1 articles about ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1200041-07-1
ethyl (S)-5-(4-(benzyloxy)phenyl)-4-(tert-butoxycarbonylamino)-2-en-2-methylpentanoate

: 1200041-09-3
ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate

: 1200041-26-4
ethyl (2R,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 24h;
DOI:10.1021/ol902320w

Reference yield: 88.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 1200041-09-3
ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate

: ethyl (2S,4R)-4-[(tert-butoxycarbonyl)amino]-2-methyl-5-(4-{[(trifluoromethyl)sulfonyl]oxy}phenyl)pentanoate

Guidance literature:: With triethylamine; In dichloromethane; at 200 ℃;

Reference yield:

: 1200041-09-3
ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate

: 1200041-11-7
tubutyrosine hydrochloride

Guidance literature:: ethyl (2S,4R)-5-(4-(hydroxy)phenyl)-4-(tert-butoxycarbonylamino)-2-methylpentanoate; With lithium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃;

With hydrogenchloride; water; In ethyl acetate; at 20 ℃; for 2h;
DOI:10.1021/ol902320w