2-(3,7-dimethylocta-2,6-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3,7-dimethylocta-2,6-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1057662-85-7
Molecular Formula:C₁₆H₂₉BO₂
Molecular Weight:264.216
Hs Code.:

Synonyms:2-(3,7-dimethylocta-2,6-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Suppliers and Price of 2-(3,7-dimethylocta-2,6-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 18 raw suppliers

Chemical Property of 2-(3,7-dimethylocta-2,6-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property:

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 2-(3,7-dimethylocta-2,6-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about 2-(3,7-dimethylocta-2,6-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5389-87-7
1-chloro-3,7-dimethylocta-2,6-diene

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1174918-99-0
2-(3,7-dimethylocta-1,6-dien-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1057662-85-7
2-(3,7-dimethylocta-2,6-dienyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With bis(trifluoromethane)sulfonimide lithium; In tetrahydrofuran; byproducts: HCl; Electrolysis; geranyl chloride (1 mmol) and pinacolborane (3 mmol) added to THF containing 0.7 M (CF3SO2)2NLi under N2; electrolyzed with Al anode and Ni cathode (room temp., const. c.d. of 0.15 A/dm2) to 2-3 F/mol; evapd. (vac.); hydrolyzed with H2O; extd. with Et2O; org. phase washed with H2O and satd. aq. NaCl; dried over MgSO4; concd. (vac.); pyrified bycolumn chromy. (silica-gel, petroleum ether-Et2O);
DOI:10.1016/j.electacta.2009.01.015

Reference yield: 95.0%

: 1057662-85-7
(E)-2-(3,7-dimethylocta-2,6-dien-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 41492-05-1
p-bromobutylbenzene

: C₂₀H₃₀

Guidance literature:: With potassium phosphate; bis(η3-allyl-μ-chloropalladium(II)); dicyclohexyl(2-(2-methoxynaphthalen-1-yl)phenyl)phosphine; In water; acetonitrile; at 40 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja405950c

Reference yield: 82.0%

: 1057662-85-7
(E)-2-(3,7-dimethylocta-2,6-dien-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1544322-28-2
(E)-1-(5-iodo-2,4-bis(methoxymethoxy)phenyl)-3-(4 (methoxymethoxy)phenyl)prop-2-en-1-one

: 1544322-48-6
(E)-1-(5-((E)-3,7-dimethylocta-2,6-dien-1-yl)-2,4-bis(methoxymethoxy)phenyl)-3-(4-(methoxymethoxy)phenyl)prop-2-en-1-one

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 2h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.tetlet.2013.12.044