1,2,4-Trioxolane,3,5-bis(chloromethyl)-3-methyl-5-(2-propenyl)-,(3R,5R)-rel-(9CI)

Base Information

• Chemical Name: 1,2,4-Trioxolane,3,5-bis(chloromethyl)-3-methyl-5-(2-propenyl)-,(3R,5R)-rel-(9CI)
• CAS No.: 783340-76-1
• Molecular Formula: C₈H₁₂Cl₂O₃
• Molecular Weight: 227.087
• Mol file: 783340-76-1.mol

Synonyms:1,2,4-Trioxolane,3,5-bis(chloromethyl)-3-methyl-5-(2-propenyl)-, (3R,5R)-rel- (9CI)

Chemical Property of 1,2,4-Trioxolane,3,5-bis(chloromethyl)-3-methyl-5-(2-propenyl)-,(3R,5R)-rel-(9CI)

Chemical Property:

• PSA: 27.69000
• LogP: 2.43100

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2,4-Trioxolane,3,5-bis(chloromethyl)-3-methyl-5-(2-propenyl)-,(3R,5R)-rel-(9CI)

There total 2 articles about 1,2,4-Trioxolane,3,5-bis(chloromethyl)-3-methyl-5-(2-propenyl)-,(3R,5R)-rel-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

allyl-trimethyl-silane (762-72-1) + 1,2,4-trichloro-3-methyl-2-butene → cis-3-allyl-3,5-bis(chloromethyl)-5-methyl-1,2,4-trioxolane (783340-76-1) + trans-3-allyl-3,5-bis(chloromethyl)-5-methyl-1,2,4-trioxolane (783340-76-1)

Guidance literature:

1,2,4-trichloro-3-methyl-2-butene; With ozone; In pentane; at -78 ℃;

allyl-trimethyl-silane; With titanium tetrachloride; In dichloromethane; at -75 ℃; for 2h; Further stages.;

DOI:10.1002/ejoc.200400167

Reference yield: 21.0%

allyl-trimethyl-silane (762-72-1) + 1,2,4-trichloro-3-methyl-2-butene → cis-3-allyl-3,5-bis(chloromethyl)-5-methyl-1,2,4-trioxolane (783340-76-1) + trans-3-allyl-3,5-bis(chloromethyl)-5-methyl-1,2,4-trioxolane (783340-76-1)

Guidance literature:

1,2,4-trichloro-3-methyl-2-butene; With ozone; In pentane; at -78 ℃;

allyl-trimethyl-silane; With titanium tetrachloride; In dichloromethane; at -75 ℃; for 2h; Further stages.;

DOI:10.1002/ejoc.200400167

upstream raw materials:

allyl-trimethyl-silane

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