β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide

Base Information

Chemical Name:β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide
CAS No.:129749-00-4
Molecular Formula:BrH*C₁₈H₁₈N₂O₄
Molecular Weight:407.264
Hs Code.:

Synonyms:β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide

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Chemical Property of β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide

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Technology Process of β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide

There total 3 articles about β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 129748-99-8
N^α-Cbz-β-carboxymethyl-N-(2'-benzoylphenyl)aspartamide

: 129749-00-4
β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide

Guidance literature:: With hydrogen bromide; In dichloromethane; Ambient temperature; 1) 20 min, 2) 4h (procedure 2x);

Reference yield:

: 3160-47-2
N-(benzyloxycarbonyl)-L-aspartic acid 4-methyl ester

: 129749-00-4
β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) N-methylmorpholine, isobutylchloroformate / 1) methylene chloride, 0 deg C to r.t., 10 min, 2) methylene chloride, reflux, 20 min, then r.t., 69h

2: 75 percent / HBr / CH₂Cl₂ / Ambient temperature; 1) 20 min, 2) 4h (procedure 2x)

With 4-methyl-morpholine; hydrogen bromide; isobutyl chloroformate; In dichloromethane;

Reference yield:

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: 129749-00-4
β-Carboxymethyl-N-(2'-benzoylphenyl)aspartamide hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) N-methylmorpholine, isobutylchloroformate / 1) methylene chloride, 0 deg C to r.t., 10 min, 2) methylene chloride, reflux, 20 min, then r.t., 69h

2: 75 percent / HBr / CH₂Cl₂ / Ambient temperature; 1) 20 min, 2) 4h (procedure 2x)

With 4-methyl-morpholine; hydrogen bromide; isobutyl chloroformate; In dichloromethane;