Technology Process of C28H29N7O2
There total 5 articles about C28H29N7O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
hexane; toluene;
at -78 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ja502780z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / Inert atmosphere
2: diisobutylaluminium hydride / toluene; hexane / 2 h / -78 °C / Inert atmosphere
With
diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja502780z
- Guidance literature:
-
Multi-step reaction with 5 steps
1: rhodium(II) acetate dimer / dichloromethane / 10 h / Inert atmosphere
2: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
3: triphenylphosphine / tetrahydrofuran; water / 10 h / 20 °C / Inert atmosphere
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / Inert atmosphere
5: diisobutylaluminium hydride / toluene; hexane / 2 h / -78 °C / Inert atmosphere
With
sodium azide; rhodium(II) acetate dimer; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja502780z