Technology Process of 1-(α-imino-2',4',6'-trimethylbenzyl)-2-hydroxy-2,3,3-trimethyl-indoline
There total 5 articles about 1-(α-imino-2',4',6'-trimethylbenzyl)-2-hydroxy-2,3,3-trimethyl-indoline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / Et3N / benzene / 24 h / Ambient temperature
2: 76 percent / hydrogen / W-2 Raney nickel / methanol / 760 Torr / Ambient temperature
3: toluene / 5 h / Heating
4: 95 percent / CHCl3 / Ambient temperature
5: 92 percent / hydrogen / W-2 Raney nickel / methanol / 760 Torr / Ambient temperature
With
hydrogen; triethylamine;
W-2 Raney nickel;
In
methanol; chloroform; toluene; benzene;
DOI:10.1016/S0040-4020(01)90084-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 20 percent / 30percent hydrochloric acid / methanol / 25 h / Heating
2: 95 percent / CHCl3 / Ambient temperature
3: 92 percent / hydrogen / W-2 Raney nickel / methanol / 760 Torr / Ambient temperature
With
hydrogenchloride; hydrogen;
W-2 Raney nickel;
In
methanol; chloroform;
DOI:10.1016/S0040-4020(01)90084-5