1,1-dimethylethyl ((1S)-1-{[(2-fluoro-4-iodophenyl)amino]carbonyl}-3-hydroxypropyl)-carbamate

Base Information

Chemical Name:1,1-dimethylethyl ((1S)-1-{[(2-fluoro-4-iodophenyl)amino]carbonyl}-3-hydroxypropyl)-carbamate
CAS No.:553652-15-6
Molecular Formula:C₁₅H₂₀FIN₂O₄
Molecular Weight:438.238
Hs Code.:

Synonyms:1,1-dimethylethyl ((1S)-1-{[(2-fluoro-4-iodophenyl)amino]carbonyl}-3-hydroxypropyl)-carbamate

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Chemical Property of 1,1-dimethylethyl ((1S)-1-{[(2-fluoro-4-iodophenyl)amino]carbonyl}-3-hydroxypropyl)-carbamate

Chemical Property:

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Technology Process of 1,1-dimethylethyl ((1S)-1-{[(2-fluoro-4-iodophenyl)amino]carbonyl}-3-hydroxypropyl)-carbamate

There total 2 articles about 1,1-dimethylethyl ((1S)-1-{[(2-fluoro-4-iodophenyl)amino]carbonyl}-3-hydroxypropyl)-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29632-74-4
2-fluro-4-iodoaniline

: 40856-59-5,132957-40-5
tert-butyl (3S)-2-oxotetrahydrofuran-3-ylcarbamate

: 553652-15-6
1,1-dimethylethyl ((1S)-1-{[(2-fluoro-4-iodophenyl)amino]carbonyl}-3-hydroxypropyl)-carbamate

Guidance literature:: 2-fluro-4-iodoaniline; In n-heptane; dichloromethane; at 0 ℃; for 0.5h;

tert-butyl (3S)-2-oxotetrahydrofuran-3-ylcarbamate; In n-heptane; dichloromethane; at 0 - 18 ℃; for 18h;

Reference yield:

: 40856-59-5,132957-40-5
tert-butyl (3S)-2-oxotetrahydrofuran-3-ylcarbamate

: 553652-15-6
1,1-dimethylethyl ((1S)-1-{[(2-fluoro-4-iodophenyl)amino]carbonyl}-3-hydroxypropyl)-carbamate

Guidance literature:: 2-fluro-4-iodoaniline; With trimethylaluminum; In n-heptane; dichloromethane; at 0 ℃; for 0.5h;

tert-butyl (3S)-2-oxotetrahydrofuran-3-ylcarbamate; In dichloromethane; at 0 - 20 ℃; for 18h;

With citric acid; In water;