(E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime

Base Information

• Chemical Name: (E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime
• CAS No.: 1390649-34-9
• Molecular Formula: C₂₇H₂₄N₄O₃
• Molecular Weight: 452.513

Synonyms:(E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime

Chemical Property of (E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime

Chemical Property:

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Technology Process of (E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime

There total 3 articles about (E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

6-(3-acetylphenylamino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one (1135212-96-2) + N-methoxylamine hydrochloride (593-56-6) → (E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime (1390649-34-9)

Guidance literature:

In 2-ethoxy-ethanol; for 0.5h; Microwave irradiation;

DOI:10.1016/j.bmc.2012.05.035

Reference yield:

1-(3-aminophenyl)ethanone (99-03-6) → (E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime (1390649-34-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / 2-ethoxy-ethanol / 1 h / Microwave irradiation

2: 2-ethoxy-ethanol / 0.5 h / Microwave irradiation

With potassium carbonate; In 2-ethoxy-ethanol;

DOI:10.1016/j.bmc.2012.05.035

Reference yield:

6-chloro-9-methoxy-11H-indeno[1,2-c]quinolin-11-one (191801-89-5) → (E)-9-methoxy-6-((3-[(E)-1-(methoximino)ethyl]phenyl)amino)-11H-indeno[1,2-c]quinolin-11-one O-methyloxime (1390649-34-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / 2-ethoxy-ethanol / 1 h / Microwave irradiation

2: 2-ethoxy-ethanol / 0.5 h / Microwave irradiation

With potassium carbonate; In 2-ethoxy-ethanol;

DOI:10.1016/j.bmc.2012.05.035

upstream raw materials:

6-chloro-9-methoxy-11H-indeno[1,2-c]quinolin-11-one

6-(3-acetylphenylamino)-9-methoxy-11H-indeno[1,2-c]quinolin-11-one

N-methoxylamine hydrochloride

1-(3-aminophenyl)ethanone

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