(Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester

Base Information

Chemical Name:(Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester
CAS No.:434331-74-5
Molecular Formula:C₃₀H₃₁NO₄
Molecular Weight:469.58
Hs Code.:

Synonyms:(Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester

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Technology Process of (Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester

There total 1 articles about (Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 434331-68-7
2-(benzhydrylidene-amino)-pent-2-enedioic acid 1-tert-butyl ester 5-methyl ester

: 434331-74-5
(Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In acetonitrile; for 1h;
DOI:10.1021/jo0159800

Reference yield: 85.0%

: 434331-74-5
(Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester

: 434331-82-5
5-benzyl-6-oxo-1,4,5,6-tetrahydropyridazine-3-carboxylic acid tert-butyl ester

Guidance literature:: With hydrazine hydrochloride; sodium acetate; In ethanol; for 24h; Heating;
DOI:10.1021/jo0159800

Reference yield:

: 434331-74-5
(Z)-2-(benzhydrylideneamino)-4-benzylpent-2-enedioic acid 1-tert-butyl 5-methyl ester

: 434331-90-5
5-benzyl-1-tert-butoxycarbonylmethyl-6-oxo-1,4,5,6-tetrahydropyridazine-3-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / hydrazine hydrochloride; AcONa / ethanol / 24 h / Heating

2: 90 percent / LiHMDS / tetrahydrofuran / 20 h / -78 °C

With hydrazine hydrochloride; sodium acetate; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol;
DOI:10.1021/jo0159800