tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate

Base Information

• Chemical Name: tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate
• CAS No.: 272770-37-3
• Molecular Formula: C₃₀H₅₁N₃O₇
• Molecular Weight: 565.751

Synonyms:tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate

Chemical Property of tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate

Chemical Property:

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Technology Process of tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate

There total 8 articles about tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

tert-Butyl 2,6-di-tert-butyl-4-(15-methanesulphonyl-4,7,10,13-tetraoxapentadecyl) phenyl carbonate → tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate (272770-37-3)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide;

Reference yield: 92.0%

methanesulfonic acid 2-[2-(2-{2-[3-(4-tert-butoxycarbonyloxy-3,5-di-tert-butyl-phenyl)-propoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl ester (272770-36-2) → tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate (272770-37-3)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide;

Reference yield:

methanesulfonic acid 2-[2-(2-{2-[3-(4-tert-butoxycarbonyloxy-3,5-di-tert-butyl-phenyl)-propoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl ester (272770-36-2) → tert-butyl 2,6-di-tert-butyl-4-(15-azido-4,7,10,13-tetraoxapentadecyl)phenyl carbonate (272770-37-3)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 90 ℃;

DOI:10.1016/S0960-894X(02)00698-4

upstream raw materials:

methanesulfonic acid 2-[2-(2-{2-[3-(4-tert-butoxycarbonyloxy-3,5-di-tert-butyl-phenyl)-propoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl ester

Tetraethylene glycol

di-tert-butyl dicarbonate

4-(3-Iodopropyl)-2, 6-di-tert-butylphenol

Downstream raw materials:

tert-Butyl 4-(15-(1,4-dihydro-3-hydroxy-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13-tetraoxapentadecyl)-2, 6-di-tert-butylphenyl carbonate

tert-butyl 4-(15-(3-benzyloxy-1,4-dihydro-2-methyl-4-oxo-1-pyridinyl)-4,7,10,13-tetraoxapentadecyl)-2,6-di-tert-butylphenyl carbonate

tert-butyl 2,6-di-tert-butyl-4-(15-amino-4,7,10,13-tetraoxapentadecyl)phenyl carbonate

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