2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole

Base Information

Chemical Name:2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole
CAS No.:213738-68-2
Molecular Formula:C₂₉H₃₁N₃O₆Si
Molecular Weight:545.667
Hs Code.:

Synonyms:2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole

Suppliers and Price of 2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole

There total 1 articles about 2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1825-61-2
Trimethylmethoxysilane

: 194232-63-8
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde

: 213738-68-2
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 ℃;
DOI:10.1016/S0040-4039(98)01298-2

Reference yield:

: 213738-68-2
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole

: (5S,6R)-6-[2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazol-4-yl]-3,4-dihydroxy-6-methoxy-5-methyl-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃*OEt₂ / CH₂Cl₂ / 0 deg C to rt

2: OsO₄, TMANO

With osmium(VIII) oxide; trimethylamine-N-oxide; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(98)01298-2

Reference yield:

: 213738-68-2
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-dimethoxymethyl-[2,4';2',4'']teroxazole

: 213738-57-9
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-4-((1R,2R)-2-[1,3]dithian-2-yl-1-methoxy-propyl)-[2,4';2',4'']teroxazole

Guidance literature:: Multi-step reaction with 4 steps

1: BF₃*OEt₂ / CH₂Cl₂ / 0 deg C to rt

2: OsO₄, TMANO

3: Pb(OAc)4

4: 99 percent / BF₃*OEt₂

With lead(IV) acetate; osmium(VIII) oxide; trimethylamine-N-oxide; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(98)01298-2