2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde

Base Information

Chemical Name:2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde
CAS No.:194232-63-8
Molecular Formula:C₂₇H₂₅N₃O₅Si
Molecular Weight:499.598
Hs Code.:

Synonyms:2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde

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Chemical Property of 2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde

Chemical Property:

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Technology Process of 2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde

There total 9 articles about 2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 194232-62-7
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carboxylic acid ethyl ester

: 194232-63-8
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 ℃; for 0.116667h;
DOI:10.1016/S0040-4039(97)01218-5

Reference yield:

: 132629-37-9
ethyl 2-[(E)-2-phenylethenyl]oxazole-4-carboxylate

: 194232-63-8
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 9 steps

1: 100 percent / aq. NH₄OH / Ambient temperature

2: 1.) NaHCO₃; 2.) TFAA / 1.) THF; 2.) THF

3: TNANO / OsO₄

4: Pb(OAc)4

5: NaBH₄ / ethanol / 0 °C

6: NH₄OH

7: imidazole

8: 1.) NaHCO₃; 2.) TFAA / 1.) THF; 2.) THF

9: 85 percent / DIBAL-H / toluene / 0.12 h / -78 °C

With 1H-imidazole; lead(IV) acetate; ammonium hydroxide; sodium tetrahydroborate; diisobutylaluminium hydride; sodium hydrogencarbonate; trifluoroacetic anhydride; osmium(VIII) oxide; In ethanol; toluene;
DOI:10.1016/S0040-4039(97)01218-5

Reference yield:

: 194232-57-0
2-((E)-Styryl)-oxazole-4-carboxylic acid amide

: 194232-63-8
2''-(tert-Butyl-diphenyl-silanyloxymethyl)-[2,4';2',4'']teroxazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) NaHCO₃; 2.) TFAA / 1.) THF; 2.) THF

2: TNANO / OsO₄

3: Pb(OAc)4

4: NaBH₄ / ethanol / 0 °C

5: NH₄OH

6: imidazole

7: 1.) NaHCO₃; 2.) TFAA / 1.) THF; 2.) THF

8: 85 percent / DIBAL-H / toluene / 0.12 h / -78 °C

With 1H-imidazole; lead(IV) acetate; ammonium hydroxide; sodium tetrahydroborate; diisobutylaluminium hydride; sodium hydrogencarbonate; trifluoroacetic anhydride; osmium(VIII) oxide; In ethanol; toluene;
DOI:10.1016/S0040-4039(97)01218-5