rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine

Base Information

• Chemical Name: rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine
• CAS No.: 1394174-98-1
• Molecular Formula: C₁₇H₂₀F₃N₃
• Molecular Weight: 323.361

Synonyms:rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine

Chemical Property of rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine

Chemical Property:

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Technology Process of rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine

There total 3 articles about rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-ethyl-5-methyl-2H-pyrazol-3-yl)-ethylamine (955403-37-9) + 2-(4-(trifluoromethyl)phenyl)acetaldehyde (30934-62-4) → rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine (1394174-98-1)

Guidance literature:

With acetic acid; In ethanol; at 130 ℃; for 0.1h; under 10501.1 Torr; Microwave irradiation;

DOI:10.1016/j.bmcl.2010.01.070

Reference yield:

C17H18F3N3 → rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine (1394174-98-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃;

DOI:10.1016/j.bmcl.2010.01.070

Reference yield:

→ rac-1-ethyl-3-methyl-4-(4-trifluoromethylbenzyl)-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine (1394174-98-1)

Guidance literature:

upstream raw materials:

2-(2-ethyl-5-methyl-2H-pyrazol-3-yl)-ethylamine

2-(4-(trifluoromethyl)phenyl)acetaldehyde

Downstream raw materials:

C₂₆H₂₉F₃N₄O

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