2,4-O-benzylidene-D-tetraose

Base Information

• Chemical Name: 2,4-O-benzylidene-D-tetraose
• CAS No.: 909277-52-7
• Molecular Formula: C₁₁H₁₂O₄
• Molecular Weight: 208.214
• Mol file: 909277-52-7.mol

Synonyms:2,4-O-benzylidene-D-tetraose

Chemical Property of 2,4-O-benzylidene-D-tetraose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-O-benzylidene-D-tetraose

There total 1 articles about 2,4-O-benzylidene-D-tetraose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2,4-O-benzylidene-D-tetraose (909277-52-7)

Guidance literature:

Reference yield: 99.0%

trimethyl phosphonoacetate (5927-18-4) + 2,4-O-benzylidene-D-tetraose (909277-52-7) → C14H16O5

Guidance literature:

trimethyl phosphonoacetate; With sodium hydride; In tetrahydrofuran; at -20 ℃; for 0.5h;

2,4-O-benzylidene-D-tetraose; In tetrahydrofuran; at -20 - 20 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran; water;

Reference yield: 99.0%

dimethoxyphosphoryl-acetic acid methyl ester + 2,4-O-benzylidene-D-tetraose (909277-52-7) → C14H16O5 (942067-44-9)

Guidance literature:

dimethoxyphosphoryl-acetic acid methyl ester; With sodium hydride; In tetrahydrofuran; at -20 ℃; for 0.5h;

2,4-O-benzylidene-D-tetraose; In tetrahydrofuran; at -20 - 20 ℃; Further stages.;

DOI:10.1021/ja0715142

Downstream raw materials:

(2R,3R,4R)-1,3-O-benzylidene-1,2,3,4-octadecanetetrol

(2R,3R,4S)-1,3-O-benzylidene-1,2,3,4-octadecanetetrol

(1S)-2,4-O-benzylidene-1-C-(dimethoxyphosphinyl)-D-threitol

(1R)-2,4-O-benzylidene-1-C-(dimethoxyphosphinyl)-D-threitol