3, 3’-((1E,1’E)-(ethane-1,2-diylbis(azanylylidene))bis-(methanylylidene))diphenol

Base Information

• Chemical Name: 3, 3’-((1E,1’E)-(ethane-1,2-diylbis(azanylylidene))bis-(methanylylidene))diphenol
• CAS No.: 113940-19-5
• Molecular Formula: C₁₆H₁₆N₂O₂
• Molecular Weight: 268.315

Synonyms:3, 3’-((1E,1’E)-(ethane-1,2-diylbis(azanylylidene))bis-(methanylylidene))diphenol

Chemical Property of 3, 3’-((1E,1’E)-(ethane-1,2-diylbis(azanylylidene))bis-(methanylylidene))diphenol

Chemical Property:

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Technology Process of 3, 3’-((1E,1’E)-(ethane-1,2-diylbis(azanylylidene))bis-(methanylylidene))diphenol

There total 3 articles about 3, 3’-((1E,1’E)-(ethane-1,2-diylbis(azanylylidene))bis-(methanylylidene))diphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

meta-hydroxybenzaldehyde (100-83-4) + ethylenediamine (107-15-3,85404-18-8) → N1,N2-bis(3-Hydroxybenzylidene)ethane-1,2-diamine (113940-19-5)

Guidance literature:

In acetonitrile; at 22 ℃; for 0.75h; Inert atmosphere;

DOI:10.1021/om2008056

Reference yield: 88.0%

meta-hydroxybenzaldehyde (100-83-4) + ethylenediamine (107-15-3,85404-18-8) → 3, 3’-((1E,1’E)-(ethane-1,2-diylbis(azanylylidene))bis-(methanylylidene))diphenol (113940-19-5)

Guidance literature:

With iron(III) chloride; In methanol; at 20 ℃; for 0.5h;

DOI:10.3762/bjoc.6.134

Reference yield:

meta-hydroxybenzaldehyde (100-83-4) → 3, 3’-((1E,1’E)-(ethane-1,2-diylbis(azanylylidene))bis-(methanylylidene))diphenol (113940-19-5)

Guidance literature:

With potassium hydroxide; sodium acetate;

upstream raw materials:

meta-hydroxybenzaldehyde

ethylenediamine

Downstream raw materials:

(((CH₃)2CH)2POC₆H₄CHN)2(CH₂)2

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