N^α-(benzyloxycarbonyl)-N^δ-(carboxymethyl)-N^δ-(trifluoroacetyl)-L-ornithine

Base Information

• Chemical Name: N^α-(benzyloxycarbonyl)-N^δ-(carboxymethyl)-N^δ-(trifluoroacetyl)-L-ornithine
• CAS No.: 132343-96-5
• Molecular Formula: C₁₇H₁₉F₃N₂O₇
• Molecular Weight: 420.342

Synonyms:N^α-(benzyloxycarbonyl)-N^δ-(carboxymethyl)-N^δ-(trifluoroacetyl)-L-ornithine

Chemical Property of N^α-(benzyloxycarbonyl)-N^δ-(carboxymethyl)-N^δ-(trifluoroacetyl)-L-ornithine

Chemical Property:

Purity/Quality:

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Technology Process of N^α-(benzyloxycarbonyl)-N^δ-(carboxymethyl)-N^δ-(trifluoroacetyl)-L-ornithine

There total 2 articles about N^α-(benzyloxycarbonyl)-N^δ-(carboxymethyl)-N^δ-(trifluoroacetyl)-L-ornithine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nα-benzyloxycarbonyl-L-ornithine (2640-58-6) → Nα-(benzyloxycarbonyl)-Nδ-(carboxymethyl)-Nδ-(trifluoroacetyl)-L-ornithine (132343-96-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) 1 N aq. NaOH, 2.) NaCNBH₃, AcOH / 1.) MeOH, 2.) MeOH, pH 7.00, 2 d

2: Et₃N / methanol / 120 h / 25 °C

With sodium hydroxide; sodium cyanoborohydride; acetic acid; triethylamine; In methanol;

DOI:10.1021/jm00108a032

Reference yield:

ethyl trifluoroacetate, (383-63-1) + Nα-(benzyloxycarbonyl)-Nδ-(carboxymethyl)-L-ornithine (132343-95-4) → Nα-(benzyloxycarbonyl)-Nδ-(carboxymethyl)-Nδ-(trifluoroacetyl)-L-ornithine (132343-96-5)

Guidance literature:

With triethylamine; In methanol; at 25 ℃; for 120h;

DOI:10.1021/jm00108a032

upstream raw materials:

ethyl trifluoroacetate,

N^α-(benzyloxycarbonyl)-N^δ-(carboxymethyl)-L-ornithine

Nα-benzyloxycarbonyl-L-ornithine

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