tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane

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Chemical Name:tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane
CAS No.:154410-54-5
Molecular Formula:C₂₁H₃₄O₄Si
Molecular Weight:378.584
Hs Code.:

Synonyms:tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane

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Chemical Property of tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane

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Technology Process of tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane

There total 2 articles about tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 55145-45-4
4-(tert-butyldimethylsilyloxy)cyclohexanone

: 154410-45-4
(4-methoxyphenyl)ethanediol bis(trimethylsilyl) ether

: 154410-54-5
tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane

Guidance literature:: trimethylsilyl iodide; In dichloromethane; at -78 - 0 ℃;
DOI:10.1016/0040-4039(94)88161-8

Reference yield:

: 32345-64-5,147159-72-6,147254-29-3,13603-63-9
1-(4-methoxyphenyl) ethane-1,2-diol

: 154410-54-5
tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃

2: 82 percent / TMSI / CH₂Cl₂ / -78 - 0 °C

With triethylamine; trimethylsilyl iodide; In dichloromethane;
DOI:10.1016/0040-4039(94)88161-8

Reference yield: 90.0%

: 154410-54-5
tert-Butyl-[2-(4-methoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yloxy]-dimethyl-silane

: 55145-45-4
4-(tert-butyldimethylsilyloxy)cyclohexanone

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; for 3h; Ambient temperature;
DOI:10.1016/0040-4039(94)88161-8