methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal

Base Information

Chemical Name:methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal
CAS No.:252000-94-5
Molecular Formula:C₂₉H₄₂O₅Si₂
Molecular Weight:526.82
Hs Code.:

Synonyms:methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal

Suppliers and Price of methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal

There total 3 articles about methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 351900-86-2
methyl 3-O-(tert-butyldimethylsilyl)-glucuronate-D-glycal

: 252000-94-5
methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 100 ℃; for 4h;
DOI:10.1021/ja992608h

Reference yield:

: 57690-62-7
methyl 3,4-di-O-acetyl-1,2-dideoxy-D-arabino-hex-1-enopyranuronate

: 252000-94-5
methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / NaOMe / methanol / 1 h / 20 °C

2: imidazole / dimethylformamide / 2 h / 20 °C

3: imidazole / dimethylformamide / 4 h / 100 °C

With 1H-imidazole; sodium methylate; In methanol; N,N-dimethyl-formamide; 1: Deacetylation / 2: silylation / 3: silylation;
DOI:10.1021/ja992608h

Reference yield:

: 95530-80-6
methyl 1,2-dideoxy-D-arabino-hex-1-enopyranuronate

: 252000-94-5
methyl (3-O-tert-butyldimethylsilyl-4-O-tert-butyldiphenylsilyl-D-glucuronate)glycal

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 2 h / 20 °C

2: imidazole / dimethylformamide / 4 h / 100 °C

With 1H-imidazole; In N,N-dimethyl-formamide; 1: silylation / 2: silylation;
DOI:10.1021/ja992608h