(3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine

Base Information

Chemical Name:(3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine
CAS No.:438207-07-9
Molecular Formula:C₂₅H₃₁N₂OPSi
Molecular Weight:434.593
Hs Code.:

Synonyms:(3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine

Suppliers and Price of (3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine

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Technology Process of (3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine

There total 2 articles about (3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 22751-68-4,60508-97-6,60509-62-8,70749-06-3,118628-68-5
(S,S)-N,N'-dimethyl-1,2-diphenylethane-1,2-diamine

: 84998-49-2
2-[bis(dimethylamino)phosphanyl]phenyl trimethylsilyl ether

: 438207-07-9
(3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine

Guidance literature:: In toluene; for 2h; Heating;
DOI:10.1016/S0022-328X(01)01314-6

Reference yield:

: C₁₀H₁₆N₂OP^(1-)*Li⁽¹⁺⁾

: 438207-07-9
(3S,4S)-2,5-dimethyl-1-(2-trimethylsiloxyphenyl)-2,5-diaza-4-phospholidine

Guidance literature:: Multi-step reaction with 2 steps

1: hexane; diethyl ether / 1 h / 20 °C

2: 43 percent / toluene / 2 h / Heating

In diethyl ether; hexane; toluene;
DOI:10.1016/S0022-328X(01)01314-6