2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone

Base Information

Chemical Name:2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone
CAS No.:1374458-98-6
Molecular Formula:C₂₄H₃₂N₂O₁₁
Molecular Weight:524.525
Hs Code.:

Synonyms:2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone

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Chemical Property of 2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone

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Technology Process of 2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone

There total 3 articles about 2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1374458-97-5
3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octose (benzyloxycarbonyl)hydazone

: 1374458-98-6
2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone

Guidance literature:: 3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octose (benzyloxycarbonyl)hydazone; With hydrogenchloride; sodium cyanoborohydride; In methanol; dichloromethane; water; pH=1 - 3;

With sodium hydrogencarbonate; In methanol; dichloromethane;
DOI:10.1016/j.tetlet.2012.03.072

Reference yield:

: 201279-58-5
1-deoxy-1-allyl-2,3,4,6-tetra-O-acetyl-D-galactopyranoside

: 1374458-98-6
2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone

Guidance literature:: Multi-step reaction with 3 steps

1: ozone / dichloromethane

2: toluene / 25 h / 20 - 50 °C

3: hydrogenchloride; sodium cyanoborohydride / methanol; dichloromethane; water / pH 1 - 3

With hydrogenchloride; sodium cyanoborohydride; ozone; In methanol; dichloromethane; water; toluene;
DOI:10.1016/j.tetlet.2012.03.072

Reference yield:

: 193156-88-6
2-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)acetaldehyde

: 1374458-98-6
2-[3,7-anhydro-2-deoxy-4,5,6,8-tetra-O-acetyl-D-glycero-L-gulo-octitol-1-yl]-1-(benzyloxycarbonyl)hydazone

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 25 h / 20 - 50 °C

2: hydrogenchloride; sodium cyanoborohydride / methanol; dichloromethane; water / pH 1 - 3

With hydrogenchloride; sodium cyanoborohydride; In methanol; dichloromethane; water; toluene;
DOI:10.1016/j.tetlet.2012.03.072