4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid

Base Information

Chemical Name:4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid
CAS No.:1432509-94-8
Molecular Formula:C₁₈H₁₇F₃N₂O₃
Molecular Weight:366.34
Hs Code.:

Synonyms:4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid

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Chemical Property of 4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid

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Technology Process of 4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid

There total 4 articles about 4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1432509-93-7
methyl 4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoate

: 1432509-94-8
4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid

Guidance literature:: With water; lithium hydroxide; In methanol; for 1h; Reflux;

Reference yield:

: 41189-09-7
(Z)-N'-(3,3-dimethyl-5-oxocyclohexylidene)-4-methylbenzenesulfonohydrazide

: 1432509-94-8
4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 2 h / 55 °C

1.2: 3 h / 20 °C

2.1: sodium hydride / N,N-dimethyl acetamide / 0.08 h / 20 °C

2.2: 4 h / 20 °C

3.1: lithium hydroxide; water / methanol; water / 1 h / Reflux

With water; sodium hydride; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl acetamide; water;

Reference yield:

: 908111-34-2
6,6-dimethyl-3-(trifluoromethyl)-1,5,6,7-tetrahydro-4H-indazol-4-one

: 1432509-94-8
4-((6,6-dimethyl-4-oxo-3-(trifluoromethyl)-4,5,6,7-tetrahydro-1H-indazol-1-yl)methyl)benzoaic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl acetamide / 0.08 h / 20 °C

1.2: 4 h / 20 °C

2.1: lithium hydroxide; water / methanol; water / 1 h / Reflux

With water; sodium hydride; lithium hydroxide; In methanol; N,N-dimethyl acetamide; water;