DL-2-Amino-2-methylheptansaeuremethylester

Base Information

• Chemical Name: DL-2-Amino-2-methylheptansaeuremethylester
• CAS No.: 51513-92-9
• Molecular Formula: C₉H₁₉NO₂
• Molecular Weight: 173.255
• Mol file: 51513-92-9.mol

Synonyms:DL-2-Amino-2-methylheptansaeuremethylester

Chemical Property of DL-2-Amino-2-methylheptansaeuremethylester

Chemical Property:

Purity/Quality:

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Technology Process of DL-2-Amino-2-methylheptansaeuremethylester

There total 1 articles about DL-2-Amino-2-methylheptansaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

methyl 2-(2-benzoyl-2-methylhydrazinyl)-2-methylheptanoate (1029435-31-1) → N-methylbenzamide (88070-48-8) + DL-2-Amino-2-methylheptansaeuremethylester (51513-92-9)

Guidance literature:

methyl 2-(2-benzoyl-2-methylhydrazinyl)-2-methylheptanoate; With samarium diiodide; In tetrahydrofuran; methanol; at -78 - 20 ℃; for 2h; Inert atmosphere;

With acetic acid; In tetrahydrofuran; methanol; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol800733b

Reference yield:

DL-2-Amino-2-methylheptansaeuremethylester (51513-92-9) + benzoyl chloride (98-88-4) → methyl 2-benzamido-2-methylheptanoate (1029435-38-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; methanol; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol800733b

upstream raw materials:

methyl 2-(2-benzoyl-2-methylhydrazinyl)-2-methylheptanoate

Downstream raw materials:

methyl 2-benzamido-2-methylheptanoate