4-methoxyphenyl 1'-naphthalenyl selenide

Base Information

Chemical Name:4-methoxyphenyl 1'-naphthalenyl selenide
CAS No.:184034-52-4
Molecular Formula:C₁₇H₁₄OSe
Molecular Weight:313.258
Hs Code.:

Synonyms:4-methoxyphenyl 1'-naphthalenyl selenide

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Chemical Property of 4-methoxyphenyl 1'-naphthalenyl selenide

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Technology Process of 4-methoxyphenyl 1'-naphthalenyl selenide

There total 4 articles about 4-methoxyphenyl 1'-naphthalenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1787-80-0
2-bis[3,5bis(trifluoromethyl)phenyl]diselane

: 5720-07-0
4-methoxyphenylboronic acid

: 184034-52-4
4-methoxyphenyl 1'-naphthalenyl selenide

Guidance literature:: With copper(II) oxide; In dimethyl sulfoxide; at 100 ℃; for 24h; Air atmosphere;
DOI:10.1016/j.tetlet.2009.09.052

Reference yield: 62.0%

: 38762-70-8
bis(4-methoxyphenyl)diselenide

: 703-55-9
1-naphthylmagnesiumbromide

: 184034-52-4
4-methoxyphenyl 1'-naphthalenyl selenide

Guidance literature:: In diethyl ether;
DOI:10.1021/ja974070q

Reference yield:

: 90-14-2
1-Iodonaphthalene

: 184034-52-4
4-methoxyphenyl 1'-naphthalenyl selenide

Guidance literature:: Multi-step reaction with 2 steps

1: selenium; copper(I) oxide; ethylenediamine; potassium hydroxide / dimethyl sulfoxide / 18 h / 90 °C / Inert atmosphere; Sealed tube

2: copper(I) oxide; ethylenediamine; potassium hydroxide / dimethyl sulfoxide / 12 h / 110 °C / Sealed tube

With copper(I) oxide; selenium; ethylenediamine; potassium hydroxide; In dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2015.11.062