(S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

Base Information

Chemical Name:(S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide
CAS No.:1352966-71-2
Molecular Formula:C₁₈H₃₀N₂O₂
Molecular Weight:306.448
Hs Code.:

Synonyms:(S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

Chemical Property:

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Technology Process of (S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

There total 4 articles about (S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₃₈N₂O₂Si

: 1352966-70-1
(S)-2-((R)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

: 1352966-71-2
(S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.25h; optical yield given as %de; Cooling with ice;
DOI:10.1016/j.tetasy.2011.10.022

Reference yield:

: 1352966-63-2
(S,E)-2-(benzylideneamino)-N,N,4-trimethylpentanamide

: 1352966-70-1
(S)-2-((R)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

: 1352966-71-2
(S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammonium perchlorate; triethylamine / tetrahydrofuran / 20 °C / Electrochemical reaction

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / Cooling with ice

With tetrabutyl ammonium fluoride; tetrabutylammonium perchlorate; triethylamine; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2011.10.022

Reference yield:

: 100-52-7
benzaldehyde

: 1352966-70-1
(S)-2-((R)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

: 1352966-71-2
(S)-2-((S)-2-hydroxy-2-methyl-1-phenylpropylamino)-N,N,4-trimethylpentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium sulfate / dichloromethane / 20 °C

2: tetrabutylammonium perchlorate; triethylamine / tetrahydrofuran / 20 °C / Electrochemical reaction

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / Cooling with ice

With magnesium sulfate; tetrabutyl ammonium fluoride; tetrabutylammonium perchlorate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2011.10.022