C₃₄H₅₈O₄Si₂

Base Information

Chemical Name:C₃₄H₅₈O₄Si₂
CAS No.:1240318-12-0
Molecular Formula:C₃₄H₅₈O₄Si₂
Molecular Weight:587.003
Hs Code.:

C<sub>34</sub>H<sub>58</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₄H₅₈O₄Si₂

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Chemical Property of C₃₄H₅₈O₄Si₂

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Technology Process of C₃₄H₅₈O₄Si₂

There total 17 articles about C₃₄H₅₈O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1240318-11-9
C₂₈H₄₄O₄Si

: 69739-34-0
t-butyldimethylsiyl triflate

: 1240318-12-0
C₃₄H₅₈O₄Si₂

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol1015652

Reference yield:

: 10504-05-9
5-methyl-2-(1-methylethyl)furan

: 1240318-12-0
C₃₄H₅₈O₄Si₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: rhodium (II) octanoate dimer / hexane / 6 h / Inert atmosphere; Reflux

2.1: diisobutylaluminium hydride / n-heptane; dichloromethane / 0.25 h / -78 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 0.08 h / -30 °C / Inert atmosphere

4.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1.75 h / -78 - 0 °C / Inert atmosphere

4.2: 1.75 h / -78 - 0 °C / Inert atmosphere

5.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C / Inert atmosphere

6.1: oxalic acid / methanol; dichloromethane / 0.5 h / 20 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

8.1: 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; triethylamine / 5 h / 85 °C / Inert atmosphere

9.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

10.1: sodium methylate / methanol / 0.17 h / 65 °C / Inert atmosphere

11.1: sodium tetrahydroborate / methanol / 0.25 h / 0 - 20 °C / Inert atmosphere

12.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / 0 °C / Inert atmosphere

12.2: 0.33 h / 60 °C / Inert atmosphere

13.1: borane-THF / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

13.2: 1 h / 20 °C / Inert atmosphere

14.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; borane-THF; rhodium (II) octanoate dimer; boron trifluoride diethyl etherate; sodium methylate; sodium hexamethyldisilazane; 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; oxalic acid; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; triethylamine; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; n-heptane; dichloromethane; N,N-dimethyl-formamide; mineral oil; 5.1: Rubottom oxidation / 8.1: Stetter reaction / 9.1: Aldol condensation;
DOI:10.1002/asia.201101021

Reference yield:

: C₂₁H₃₆O₄Si

: 1240318-12-0
C₃₄H₅₈O₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / methanol / 0.17 h / 65 °C / Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 0.25 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.08 h / 0 °C / Inert atmosphere

3.2: 0.33 h / 60 °C / Inert atmosphere

4.1: borane-THF / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; borane-THF; sodium methylate; sodium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/asia.201101021