N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide

Base Information

Chemical Name:N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide
CAS No.:88336-54-3
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

Synonyms:N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide

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Technology Process of N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide

There total 4 articles about N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6836-19-7
7-Methoxy-1-tetralone

: 88336-54-3
N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium tert-butoxide, isoamyl nitrite / diethyl ether; butan-1-ol / 4 h / Ambient temperature

2: H₂ / 10percent Pd/C / tetrahydrofuran

3: 55 percent / sodium borohydride / ethanol

4: dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / 1 h

With dmap; sodium tetrahydroborate; potassium tert-butylate; hydrogen; dicyclohexyl-carbodiimide; isopentyl nitrite; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; butan-1-ol;
DOI:10.1021/jm00378a014

Reference yield:

: 2471-80-9
2-hydroximino-7-methoxy-1-tetralone

: 88336-54-3
N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / tetrahydrofuran

2: 55 percent / sodium borohydride / ethanol

3: dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / 1 h

With dmap; sodium tetrahydroborate; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00378a014

Reference yield:

: 88058-66-6
N-(7-Methoxy-1-oxo-1,2,3,4-tetrahydro-naphthalen-2-yl)-propionamide

: 88336-54-3
N-[(1R,2R)-7-Methoxy-1-(3-methoxy-2-oxo-3-phenyl-propyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / sodium borohydride / ethanol

2: dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / 1 h

With dmap; sodium tetrahydroborate; dicyclohexyl-carbodiimide; In ethanol;
DOI:10.1021/jm00378a014