4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile

Base Information

Chemical Name:4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile
CAS No.:178813-96-2
Molecular Formula:C₂₆H₄₀N₂O₁₀
Molecular Weight:540.611
Hs Code.:

Synonyms:4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile

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Chemical Property of 4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile

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Technology Process of 4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile

There total 4 articles about 4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 544-92-3
copper(I) cyanide

: 178813-93-9
1,2-Dibromo-4,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzene

: 178813-96-2
4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile

Guidance literature:: In N,N-dimethyl-formamide; for 8h; Heating;
DOI:10.1021/jp960504c

Reference yield:

: 52995-76-3
1-chloro-3,6,9-trioxadecane

: 178813-96-2
4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / NaOH

2: 76 percent / Br₂, Fe, I₂ / CH₂Cl₂ / 20 h / Ambient temperature

3: 61 percent / dimethylformamide / 8 h / Heating

With sodium hydroxide; bromine; iodine; iron; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jp960504c

Reference yield:

: 10234-40-9
2,2'-(1,2-phenylenedioxy)diethanol

: 178813-96-2
4,5-Bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-phthalonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / NaOH

2: 76 percent / Br₂, Fe, I₂ / CH₂Cl₂ / 20 h / Ambient temperature

3: 61 percent / dimethylformamide / 8 h / Heating

With sodium hydroxide; bromine; iodine; iron; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jp960504c