4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one

Base Information

Chemical Name:4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one
CAS No.:258886-06-5
Molecular Formula:C₁₀H₉BrClN₃O₂
Molecular Weight:318.557
Hs Code.:

Synonyms:4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one

Chemical Property:

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Technology Process of 4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one

There total 3 articles about 4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51291-82-8
5-methoxy-1,2,4-triazol-3(2H)-one

: 149965-41-3
5-Bromo-2-chlorobenzyl bromide

: 258886-06-5
4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one

Guidance literature:: With potassium carbonate; In tert-butyl methyl ether; water; acetonitrile;

Reference yield:

: 21739-92-4
5-bromo-2-chlorobenzoic acid

: 258886-06-5
4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / tetrahydrofuran; hexane; tert-butyl methyl ether; water

2: sodium hydrogencarbonate / (2S)-N-methyl-1-phenylpropan-2-amine hydrate; diethyl ether; tert-butyl methyl ether; water

3: potassium carbonate / tert-butyl methyl ether; water; acetonitrile

With sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; diethyl ether; hexane; tert-butyl methyl ether; water; acetonitrile;

Reference yield:

: 149965-40-2
5-bromo-2-chlorobenzyl alcohol

: 258886-06-5
4-(5-bromo-2-chlorobenzyl)-5-methoxy-2,4-dihydro-3H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / (2S)-N-methyl-1-phenylpropan-2-amine hydrate; diethyl ether; tert-butyl methyl ether; water

2: potassium carbonate / tert-butyl methyl ether; water; acetonitrile

With sodium hydrogencarbonate; potassium carbonate; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; diethyl ether; tert-butyl methyl ether; water; acetonitrile;