4-Methyl-4-((Z)-6-trimethylsilanyl-hex-3-ene-1,5-diynyl)-cyclohex-2-enone

Base Information Edit

Chemical Name:4-Methyl-4-((Z)-6-trimethylsilanyl-hex-3-ene-1,5-diynyl)-cyclohex-2-enone
CAS No.:152428-88-1
Molecular Formula:C₁₆H₂₀OSi
Molecular Weight:256.42
Hs Code.:
Mol file:152428-88-1.mol

Synonyms:4-Methyl-4-((Z)-6-trimethylsilanyl-hex-3-ene-1,5-diynyl)-cyclohex-2-enone

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Chemical Property of 4-Methyl-4-((Z)-6-trimethylsilanyl-hex-3-ene-1,5-diynyl)-cyclohex-2-enone Edit

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Technology Process of 4-Methyl-4-((Z)-6-trimethylsilanyl-hex-3-ene-1,5-diynyl)-cyclohex-2-enone

There total 3 articles about 4-Methyl-4-((Z)-6-trimethylsilanyl-hex-3-ene-1,5-diynyl)-cyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-methoxy-1-methyl-4-((trimethylsilyl)oxy)cyclohex-3-enecarbaldehyde

: 152428-88-1
4-Methyl-4-((Z)-6-trimethylsilanyl-hex-3-ene-1,5-diynyl)-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 3 steps

1: tBuOK / tetrahydrofuran / 16.5 h / -78 - -9 °C

2: camphorsulfonic acid / diethyl ether / 72 h / 20 °C

3: CuI, Pd(PPh₃)4, Et₂NH / 0.25 h / 25 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; camphor-10-sulfonic acid; potassium tert-butylate; diethylamine; In tetrahydrofuran; diethyl ether;

Reference yield:

: (4-Ethynyl-3-methoxy-4-methyl-cyclohex-1-enyloxy)-trimethyl-silane

: 152428-88-1
4-Methyl-4-((Z)-6-trimethylsilanyl-hex-3-ene-1,5-diynyl)-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: camphorsulfonic acid / diethyl ether / 72 h / 20 °C

2: CuI, Pd(PPh₃)4, Et₂NH / 0.25 h / 25 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; camphor-10-sulfonic acid; diethylamine; In diethyl ether;