C₆₀H₉₀N₁₀O₁₅

Base Information

• Chemical Name: C₆₀H₉₀N₁₀O₁₅
• CAS No.: 1163732-91-9
• Molecular Formula: C₆₀H₉₀N₁₀O₁₅
• Molecular Weight: 1191.43
• Mol file: 1163732-91-9.mol

Synonyms:C₆₀H₉₀N₁₀O₁₅

Chemical Property of C₆₀H₉₀N₁₀O₁₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₉₀N₁₀O₁₅

There total 4 articles about C₆₀H₉₀N₁₀O₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

tripopargylamine (6921-29-5) + 1-(4-(azidomethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane (1163733-06-9) → C60H90N10O15 (1163732-91-9)

Guidance literature:

With 2,6-dimethylpyridine; tetrakis(acetonitrile)copper(I) hexafluorophosphate; In acetonitrile; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1039/c0cc05376g

Reference yield:

1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane (1163733-05-8) → C60H90N10O15 (1163732-91-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

2: 2,6-dimethylpyridine; tetrakis(acetonitrile)copper(I) hexafluorophosphate / acetonitrile / 72 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium azide; tetrakis(acetonitrile)copper(I) hexafluorophosphate; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1039/c0cc05376g

Reference yield:

tetraethylene glycol monomethyl ether (23783-42-8,95507-80-5) → C60H90N10O15 (1163732-91-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 110 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine; tetrakis(acetonitrile)copper(I) hexafluorophosphate / acetonitrile / 72 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium azide; tetrakis(acetonitrile)copper(I) hexafluorophosphate; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1039/c0cc05376g

upstream raw materials:

1-(4-(chloromethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane

tripopargylamine

1-(4-(azidomethyl)phenyl)-2,5,8,11,14-pentaoxapentadecane

tetraethylene glycol monomethyl ether