2-[4-[1-(3-fluoropropyl)-4-(4-pyridinyl)-1H-pyrazol-3-yl]phenoxymethyl]-6-methylpyridine hydrochloric acid

Base Information

Chemical Name:2-[4-[1-(3-fluoropropyl)-4-(4-pyridinyl)-1H-pyrazol-3-yl]phenoxymethyl]-6-methylpyridine hydrochloric acid
CAS No.:1301167-85-0
Molecular Formula:C₂₄H₂₃FN₄O*ClH
Molecular Weight:438.932
Hs Code.:

Synonyms:2-[4-[1-(3-fluoropropyl)-4-(4-pyridinyl)-1H-pyrazol-3-yl]phenoxymethyl]-6-methylpyridine hydrochloric acid

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Chemical Property of 2-[4-[1-(3-fluoropropyl)-4-(4-pyridinyl)-1H-pyrazol-3-yl]phenoxymethyl]-6-methylpyridine hydrochloric acid

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Technology Process of 2-[4-[1-(3-fluoropropyl)-4-(4-pyridinyl)-1H-pyrazol-3-yl]phenoxymethyl]-6-methylpyridine hydrochloric acid

There total 5 articles about 2-[4-[1-(3-fluoropropyl)-4-(4-pyridinyl)-1H-pyrazol-3-yl]phenoxymethyl]-6-methylpyridine hydrochloric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 462-43-1
3-fluoropropane-1-ol

: 1301167-85-0
2-[4-[1-(3-fluoropropyl)-4-(4-pyridinyl)-1H-pyrazol-3-yl]phenoxymethyl]-6-methylpyridine hydrochloric acid

Guidance literature:: With diisopropyl (E)-azodicarboxylate; triphenylphosphine; In tetrahydrofuran;

Reference yield:

: 1301167-67-8
4-[3-(4-benzyloxyphenyl)-1-(3-fluoropropyl)-1H-pyrazol-4-yl]pyridine

: 1301167-85-0
2-[4-[1-(3-fluoropropyl)-4-(4-pyridinyl)-1H-pyrazol-3-yl]phenoxymethyl]-6-methylpyridine hydrochloric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 5%-palladium/activated carbon; hydrogen / ethanol / 80 °C / 760.05 Torr

2: di-tert-butyl-diazodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.33 h / 120 °C / Microwave irradiation

3: hydrogenchloride / isopropyl alcohol

With hydrogenchloride; di-tert-butyl-diazodicarboxylate; 5%-palladium/activated carbon; hydrogen; triphenylphosphine; In tetrahydrofuran; ethanol; isopropyl alcohol;
DOI:10.1021/jm200536d