8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside

Base Information

Chemical Name:8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside
CAS No.:382607-77-4
Molecular Formula:C₅₂H₅₀BrN₅O₁₁S
Molecular Weight:1032.97
Hs Code.:

8-[O<sup>6</sup>-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside

Synonyms:8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside

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Chemical Property of 8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside

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Technology Process of 8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside

There total 5 articles about 8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.7%

: 192441-08-0
6-((4-bromothiophen-2-yl)methoxy)-9H-purin-2-amine

: 382607-65-0
8-bromooctyl-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside

: 382607-77-4
8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside

Guidance literature:: 6-((4-bromothiophen-2-yl)methoxy)-9H-purin-2-amine; With lithium hydride; In N,N-dimethyl-formamide; at 20 - 80 ℃; for 1h;

8-bromooctyl-2,3,4,6-tetra-O-benzoyl-β-D-glucopyranoside; In N,N-dimethyl-formamide; Further stages.; Heating;
DOI:10.1021/jm010006e

Reference yield:

: 18791-75-8
4-Bromothiophen-2-aldehyde

: 382607-77-4
8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 89 percent / NaBH₄ / propan-2-ol / 1 h

2.1: NaH; DMSO / 1 h

2.2: 70 percent / dimethylsulfoxide / 1 h

3.1: LiH / dimethylformamide / 1 h / 20 - 80 °C

3.2: 37.7 percent / dimethylformamide / Heating

With sodium tetrahydroborate; lithium hydride; sodium hydride; dimethyl sulfoxide; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm010006e

Reference yield:

: 114682-36-9,14218-11-2,14218-30-5,61198-88-7,108438-33-1,108836-02-8,127305-34-4,151377-77-4
β-1-bromo-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

: 382607-77-4
8-[O⁶-(4-bromothenyl)-guan-9-yl]-octyl-β-D-tetra-O-benzoylglucoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 48 percent / 3 Angstroem molecular sieves; silver phosphate / nitromethane

2.1: LiH / dimethylformamide / 1 h / 20 - 80 °C

2.2: 37.7 percent / dimethylformamide / Heating

With silver orthophosphate; 3 A molecular sieve; lithium hydride; In nitromethane; N,N-dimethyl-formamide; 1.1: Koenigs-Knorr reaction;
DOI:10.1021/jm010006e