5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene

Base Information

Chemical Name:5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene
CAS No.:853947-40-7
Molecular Formula:C₂₃H₃₀O₃
Molecular Weight:354.489
Hs Code.:

Synonyms:5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene

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Chemical Property of 5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene

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Technology Process of 5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene

There total 5 articles about 5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 853947-39-4
5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentyne

: 853947-40-7
5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene

Guidance literature:: With quinoline; Lindlar's catalyst; hydrogen; In methanol;
DOI:10.1021/jo050336x

Reference yield:

: 853947-46-3
5-(4-methoxy-2,3,6-trimethylphenyl)-3-methoxycarbonyloxy-3-methylpentyne

: 853947-40-7
5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / DBU; CuCl₂ / acetonitrile / 0 °C

2: 68 percent / Lindlar catalyst; quinoline; H₂ / methanol

With quinoline; Lindlar's catalyst; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper dichloride; In methanol; acetonitrile;
DOI:10.1021/jo050336x

Reference yield:

: 57399-32-3
4-(4-methoxy-2,3,6-trimethylphenyl)butan-2-one

: 853947-40-7
5-(4-methoxy-2,3,6-trimethylphenyl)-3-(4-methoxyphenoxy)-3-methylpentene

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / tetrahydrofuran / 2 h / -5 - 0 °C

2: 69 percent / n-BuLi / hexane; tetrahydrofuran / 0 - 20 °C

3: 49 percent / DBU; CuCl₂ / acetonitrile / 0 °C

4: 68 percent / Lindlar catalyst; quinoline; H₂ / methanol

With quinoline; Lindlar's catalyst; n-butyllithium; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; copper dichloride; In tetrahydrofuran; methanol; hexane; acetonitrile;
DOI:10.1021/jo050336x