Os(NO)(CO)(CS)(P(C₆H₅)3)2⁽¹⁺⁾*ClO₄^(1-)=[Os(NO)(CO)(CS)(P(C₆H₅)3)2]ClO₄

Base Information

Chemical Name:Os(NO)(CO)(CS)(P(C₆H₅)3)2⁽¹⁺⁾*ClO₄^(1-)=[Os(NO)(CO)(CS)(P(C₆H₅)3)2]ClO₄
CAS No.:105033-00-9
Molecular Formula:C₃₈H₃₀NO₂OsP₂S*ClO₄
Molecular Weight:916.326
Hs Code.:

Os(NO)(CO)(CS)(P(C<sub>6</sub>H<sub>5</sub>)3)2<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=[Os(NO)(CO)(CS)(P(C<sub>6</sub>H<sub>5</sub>)3)2]ClO<sub>4</sub>

Synonyms:Os(NO)(CO)(CS)(P(C₆H₅)3)2⁽¹⁺⁾*ClO₄^(1-)=[Os(NO)(CO)(CS)(P(C₆H₅)3)2]ClO₄

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Chemical Property of Os(NO)(CO)(CS)(P(C₆H₅)3)2⁽¹⁺⁾*ClO₄^(1-)=[Os(NO)(CO)(CS)(P(C₆H₅)3)2]ClO₄

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Technology Process of Os(NO)(CO)(CS)(P(C₆H₅)3)2⁽¹⁺⁾*ClO₄^(1-)=[Os(NO)(CO)(CS)(P(C₆H₅)3)2]ClO₄

There total 1 articles about Os(NO)(CO)(CS)(P(C₆H₅)3)2⁽¹⁺⁾*ClO₄^(1-)=[Os(NO)(CO)(CS)(P(C₆H₅)3)2]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 14242-05-8
silver perchlorate monohydrate

: 105032-94-8
OsCl(NO)(CS)(P(C₆H₅)3)2

: 105033-00-9
Os(NO)(CO)(CS)(P(C₆H₅)3)2⁽¹⁺⁾*ClO₄^(1-)=[Os(NO)(CO)(CS)(P(C₆H₅)3)2]ClO₄

Guidance literature:: With carbon monoxide; In tetrahydrofuran; ethanol; byproducts: AgCl; (N2); a soln. of OsCl(NO)(CS)(PPh3)2 in THF is satd. with CO, treated with a soln. of AgClO4*H2O in ethanol, the suspn. is stirred for 10 min and placed under 2 atm of CO; vessel is vented, diln. (CH2Cl2), filtration, crystn. (evapn. with subsequent addn. of hexane), filtration, washing (hexane), drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(00)99663-3