5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine

Base Information

Chemical Name:5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine
CAS No.:161109-85-9
Molecular Formula:C₄₅H₅₂N₂O₉SSi
Molecular Weight:825.067
Hs Code.:

Synonyms:5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine

Chemical Property:

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Technology Process of 5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine

There total 3 articles about 5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 161109-84-8
5'-O-dimethoxytrityl-2'-O-thexyldimethylsilyluridine

: 1005-56-7
phenylcarbonochloridothioate

: 161109-85-9
5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine

Guidance literature:: With dmap; In acetonitrile; for 20h; Ambient temperature;
DOI:10.1080/15257779408012162

Reference yield:

: 67373-56-2
chlorodimethyl(1,1,2-trimethylpropyl)silane

: 161109-85-9
5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / imidazole / pyridine / 20 h / Ambient temperature

2: 76 percent / DMAP / acetonitrile / 20 h / Ambient temperature

With 1H-imidazole; dmap; In pyridine; acetonitrile;
DOI:10.1080/15257779408012162

Reference yield:

: 81246-79-9
5'-dimethoxytrityluridine

: 161109-85-9
5'-O-dimethoxytrityl-3'-O-phenoxythiocarbonyl-2'-O-thexyldimethylsilyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / imidazole / pyridine / 20 h / Ambient temperature

2: 76 percent / DMAP / acetonitrile / 20 h / Ambient temperature

With 1H-imidazole; dmap; In pyridine; acetonitrile;
DOI:10.1080/15257779408012162