(+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide

Base Information

Chemical Name:(+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide
CAS No.:131523-34-7
Molecular Formula:C₄₀H₃₆O₇S₂
Molecular Weight:692.854
Hs Code.:

Synonyms:(+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide

Suppliers and Price of (+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of (+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide

There total 3 articles about (+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 131523-34-7
(+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / BF₃*Et₂O / CHCl₃ / 0.25 h / -40 °C

With boron trifluoride diethyl etherate; In chloroform;
DOI:10.1139/v92-267

Reference yield:

: 108-98-5
thiophenol

: 131523-34-7
(+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / BF₃*Et₂O / CHCl₃ / 0.25 h / -40 °C

With boron trifluoride diethyl etherate; In chloroform;
DOI:10.1139/v92-267

Reference yield:

: 2176-18-3
4-benzyloxy-3,5-dimethoxybenzyl alcohol

: 131523-34-7
(+/-)-trans-2-(4-Benzyloxy-3,5-dimethoxybenzyl)-3-(3,4-methylenedioxy)-α,α-bis(phenylthio)benzylbutanolide

Guidance literature:: Multi-step reaction with 2 steps

1: 14.3 g / PBr₃ / diethyl ether / 12 h / Ambient temperature

With phosphorus tribromide; In diethyl ether;
DOI:10.1248/cpb.38.1898