2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester

Base Information

• Chemical Name: 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester
• CAS No.: 899827-46-4
• Molecular Formula: C₅₂H₅₇O₁₀PSSi
• Molecular Weight: 933.144

Synonyms:2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester

Chemical Property of 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester

Chemical Property:

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Technology Process of 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester

There total 2 articles about 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

t-butyldimethylsiyl triflate (69739-34-0) + 2,4,6-tri-O-benzyl-D-myo-inositol-3-diphenylphosphate-1-O-thiocarbonic acid phenyl ester (816426-24-1) → 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester (899827-46-4)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; for 3h;

DOI:10.1021/jo060702s

Reference yield:

(+)-2,4,6-tri-O-benzyl-myo-inositol-3-phosphate (474404-92-7) → 2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester (899827-46-4)

Guidance literature:

Multi-step reaction with 2 steps

1: DMAP; pyridine / CH₂Cl₂

2: 2,6-lutidine / CH₂Cl₂ / 3 h

With pyridine; 2,6-dimethylpyridine; dmap; In dichloromethane;

DOI:10.1021/jo060702s

Reference yield:

2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-diphenylphosphate-1-O-thiocarbonic acid phenyl ester (899827-46-4) → C33H45O8PSi

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene;

DOI:10.1021/ja710348r

upstream raw materials:

t-butyldimethylsiyl triflate

2,4,6-tri-O-benzyl-D-myo-inositol-3-diphenylphosphate-1-O-thiocarbonic acid phenyl ester

(+)-2,4,6-tri-O-benzyl-myo-inositol-3-phosphate

Downstream raw materials:

2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-deoxy-3-diphenyl phosphate

2,4,6-tri-O-benzyl-D-myo-inositol-1-deoxy-3-dibenzyl phosphate

2,4,6-tri-O-benzyl-5-O-tert-butyldimethylsilyl-D-myo-inositol-1-deoxy-3-dibenzyl phosphate

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