(2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester

Base Information

Chemical Name:(2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester
CAS No.:170872-78-3
Molecular Formula:C₂₄H₂₉NO₆
Molecular Weight:427.497
Hs Code.:

Synonyms:(2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester

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Chemical Property of (2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester

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Technology Process of (2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester

There total 4 articles about (2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Methyl-N-((3R,4S)-4-methyl-5-oxo-tetrahydro-furan-3-yl)-benzenesulfonamide

: 170872-78-3
(2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aq. Ba(OH)2

2: 1.) sodium naphthalene

3: PDC / dimethylformamide

With barium dihydroxide; dipyridinium dichromate; sodium naphthalenide; In N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025

Reference yield:

: (2S,3R)-4-Hydroxy-2-methyl-3-(toluene-4-sulfonylamino)-butyric acid

: 170872-78-3
(2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium naphthalene

2: PDC / dimethylformamide

With dipyridinium dichromate; sodium naphthalenide; In N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025

Reference yield:

: (2S,3R)-3-tert-Butoxycarbonylamino-4-hydroxy-2-methyl-butyric acid benzhydryl ester

: 170872-78-3
(2S,3R)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 4-benzhydryl ester 1-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: PDC / dimethylformamide

With dipyridinium dichromate; In N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025