(2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester

Base Information

Chemical Name:(2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester
CAS No.:170872-86-3
Molecular Formula:C₁₉H₂₅NO₇
Molecular Weight:379.41
Hs Code.:

Synonyms:(2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester

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Chemical Property of (2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester

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Technology Process of (2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester

There total 6 articles about (2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,3R)-4-Hydroxy-2-methyl-3-(toluene-4-sulfonylamino)-butyric acid

: 170872-86-3
(2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) sodium naphthalene

2: PDC / dimethylformamide

4: H₂ / Pd/C

5: KF(H₂O)2

With potassium fluoride; dipyridinium dichromate; hydrogen; sodium naphthalenide; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025

Reference yield:

: 4-Methyl-N-((3R,4S)-4-methyl-5-oxo-tetrahydro-furan-3-yl)-benzenesulfonamide

: 170872-86-3
(2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester

Guidance literature:: Multi-step reaction with 6 steps

1: aq. Ba(OH)2

2: 1.) sodium naphthalene

3: PDC / dimethylformamide

5: H₂ / Pd/C

6: KF(H₂O)2

With potassium fluoride; barium dihydroxide; dipyridinium dichromate; hydrogen; sodium naphthalenide; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025

Reference yield:

: (2S,3R)-3-tert-Butoxycarbonylamino-4-hydroxy-2-methyl-butyric acid benzhydryl ester

: 170872-86-3
(2R,3S)-2-tert-Butoxycarbonylamino-3-methyl-succinic acid 1-methyl ester 4-(2-oxo-2-phenyl-ethyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1: PDC / dimethylformamide

3: H₂ / Pd/C

4: KF(H₂O)2

With potassium fluoride; dipyridinium dichromate; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/ja00140a025