phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside

Base Information

Chemical Name:phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside
CAS No.:1243310-73-7
Molecular Formula:C₃₀H₃₄O₈S₂
Molecular Weight:586.727
Hs Code.:

Synonyms:phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside

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Technology Process of phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside

There total 1 articles about phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1243310-72-6
phenyl 4,6-O-benzylidene-3-O-(2-(methylsulfonyl)ethoxy)methyl-1-thio-β-D-mannopyranoside

: 100-39-0
benzyl bromide

: 1243310-73-7
phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.tet.2010.06.007

Reference yield:

: 1243310-73-7
phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside

: 1243310-94-2
methyl 2-O-benzyl-4,6-O-benzylidene-3-O-(2-O-benzyl-4,6-O-benzylidene-β-D-mannopyranosyl)-α-D-mannopyranoside

: 1243311-01-4
methyl 2-O-benzyl-4,6-O-benzylidene-3-O-[2-O-benzyl-4,6-O-benzylidene-3-O-(2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-β-D-mannopyranosyl)-β-D-mannopyranosyl]-α-D-mannopyranoside

: 1243311-00-3
methyl 2-O-benzyl-4,6-O-benzylidene-3-O-[2-O-benzyl-4,6-O-benzylidene-3-O-(2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-α-D-mannopyranosyl)-β-D-mannopyranosyl]-α-D-mannopyranoside

Guidance literature:: With trifluoromethylsulfonic anhydride; 1,1'-sulfinylbisbenzene; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -78 - 20 ℃; for 2h; optical yield given as %de; Molecular sieve;
DOI:10.1016/j.tet.2010.06.007

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1243310-73-7
phenyl 2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-1-thio-β-D-mannopyranoside

: 1243310-83-9
methyl 2,3,4-tri-O-benzyl-6-O-(2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-β-D-mannopyranosyl)-α-D-glucopyranoside

: 1243310-82-8
methyl 2,3,4-tri-O-benzyl-6-O-(2-O-benzyl-4,6-O-benzylidene-3-O-(methylsulfonyl)ethoxymethyl-α-D-mannopyranosyl)-α-D-glucopyranoside

Guidance literature:: With trifluoromethylsulfonic anhydride; 1,1'-sulfinylbisbenzene; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -78 - -72 ℃; for 2h; optical yield given as %de; Molecular sieve;
DOI:10.1016/j.tet.2010.06.007