3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide

Base Information

Chemical Name:3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide
CAS No.:1315504-06-3
Molecular Formula:C₂₃H₃₁NO₄Si
Molecular Weight:413.589
Hs Code.:

Synonyms:3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide

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Technology Process of 3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide

There total 6 articles about 3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1315504-05-2
5-(benzyloxy)-2-(tert-butyldimethylsilyloxy)-N,N-dimethylbenzamide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1315504-06-3
3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; In tetrahydrofuran; at -78 - -60 ℃;
DOI:10.1021/ja205339p

Reference yield:

: 164161-48-2
C₁₄H₁₁ClO₃

: 1315504-06-3
3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 °C

2: dmap; triethylamine / dichloromethane

3: N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium / tetrahydrofuran / -78 - -60 °C

With dmap; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja205339p

Reference yield:

: C₁₆H₁₇NO₃

: 1315504-06-3
3-(benzyloxy)-6-(tert-butyldimethylsilyloxy)-2-formyl-N,N-dimethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane

2: N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium / tetrahydrofuran / -78 - -60 °C

With dmap; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja205339p