Technology Process of N-(adamantan-1-yl)-N'-(2,4-dinitrophenyl)propane-1,3-diamine
There total 3 articles about N-(adamantan-1-yl)-N'-(2,4-dinitrophenyl)propane-1,3-diamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydrogencarbonate / water / Saturated solution
1.2: Reflux
2.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Cooling
2.2: Cooling
3.1: potassium carbonate / acetonitrile / 48 h / Darkness
With
lithium aluminium tetrahydride; sodium hydrogencarbonate; potassium carbonate;
In
diethyl ether; water; acetonitrile;
1.2: Michael addition;
DOI:10.1016/j.ejmech.2011.08.008
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 20 °C / Cooling
1.2: Cooling
2.1: potassium carbonate / acetonitrile / 48 h / Darkness
With
lithium aluminium tetrahydride; potassium carbonate;
In
diethyl ether; acetonitrile;
DOI:10.1016/j.ejmech.2011.08.008