1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine

Base Information

• Chemical Name: 1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine
• CAS No.: 132062-46-5
• Molecular Formula: C₂₉H₃₃N₃O₇SSi
• Molecular Weight: 595.748

Synonyms:1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine

Chemical Property of 1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine

There total 3 articles about 1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-<2-Deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine (132062-45-4) + methanesulfonyl chloride (124-63-0) → 1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine (132062-46-5)

Guidance literature:

With pyridine; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1002/hlca.19910740514

Reference yield:

1-(2-deoxy-β-D-erythro-pentofuranosyl)-4-nitro-1H-pyrrolo[2,3-b]pyridine (124469-62-1) → 1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine (132062-46-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / pyridine / 8 h / Ambient temperature

2: 90 percent / pyridine / CH₂Cl₂ / 12 h / Ambient temperature

With pyridine; In dichloromethane;

DOI:10.1002/hlca.19910740514

Reference yield:

tert-butylchlorodiphenylsilane (58479-61-1) → 1-<2-Deoxy-5-O-<(1,1-dimethyl)diphenylsilyl>-3-O-mesyl-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine (132062-46-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / pyridine / 8 h / Ambient temperature

2: 90 percent / pyridine / CH₂Cl₂ / 12 h / Ambient temperature

With pyridine; In dichloromethane;

DOI:10.1002/hlca.19910740514

upstream raw materials:

1-<2-Deoxy-5-O-<(1,1-dimethylethyl)diphenylsilyl>-β-D-erythro-pentofuranosyl>-4-nitro-1H-pyrrolo<2,3-b>pyridine

methanesulfonyl chloride

1-(2-deoxy-β-D-erythro-pentofuranosyl)-4-nitro-1H-pyrrolo[2,3-b]pyridine

tert-butylchlorodiphenylsilane

Downstream raw materials:

C₁₂H₁₄N₃O₁₃P₃

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