tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate

Base Information

Chemical Name:tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate
CAS No.:1351831-45-2
Molecular Formula:C₂₂H₃₃NO₅
Molecular Weight:391.508
Hs Code.:

Synonyms:tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate

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Chemical Property of tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate

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Technology Process of tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate

There total 1 articles about tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₂₂H₃₁NO₅

: 1351831-45-2
tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate

Guidance literature:: With quinoline; hydrogen; In ethyl acetate; at 20 ℃;
DOI:10.1016/j.tet.2011.10.014

Reference yield:

: 1351831-45-2
tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate

: C₁₉H₂₉NO₅

Guidance literature:: tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate; With phosphoric acid; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃; pH=8;
DOI:10.1016/j.tet.2011.10.014

Reference yield:

: 1351831-45-2
tert-butyl ((R,Z)-4-((4R,5R)-5-benzyl-2,2-dimethyl-1,3-dioxan-4-yl)-2-hydroxybut-3-en-1-yl)carbamate

: 1351831-46-3
C₃₇H₇₁NO₅Si₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: phosphoric acid / tetrahydrofuran / 3 h / 0 - 20 °C

1.2: 0 °C / pH 8

2.1: 2,6-dimethylpyridine / dichloromethane / -78 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; phosphoric acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2011.10.014